	US 12,171,730 B2
	Hexylamine salts and methods of using hexylamine
Ronald Kramer, Signal Hills, CA (US); and Alexandros Nikolaidis, Nea Kallikratia (GR)
Assigned to ThermoLife International, LLC, Signal Hill, CA (US)
Filed by ThermoLife International, LLC, Signal Hill, CA (US)
Filed on Jan. 3, 2023, as Appl. No. 18/092,800.
Application 18/092,800 is a division of application No. 16/850,942, filed on Apr. 16, 2020, granted, now 11,541,020.
Claims priority of provisional application 62/834,878, filed on Apr. 16, 2019.
Prior Publication US 2023/0149325 A1, May 18, 2023
Int. Cl. A61K 31/131 (2006.01); A23L 33/10 (2016.01); A61K 9/00 (2006.01); A61K 31/194 (2006.01); A61K 31/522 (2006.01); A61K 45/06 (2006.01)

CPC A61K 31/131 (2013.01) [A23L 33/10 (2016.08); A61K 31/194 (2013.01); A61K 9/0053 (2013.01); A61K 31/522 (2013.01); A61K 45/06 (2013.01)]

6 Claims

1. A method of producing tri-hexylamine citrate, the method comprising:

dissolving an amount of citric acid in a solvent to produce a saturated solution of citric acid, wherein the solvent does not chemically react to citric acid or hexylamine and the citric acid and hexylamine are both soluble in the solvent; and

adding an amount of hexylamine to the saturated solution of citric acid to produce a mixture containing a precipitate, wherein the molar ratio of the amount of the hexylamine to the amount of citric acid is 3:1, wherein the amount of hexylamine is added drop by drop.