US 12,148,566 B2
Method for incorporating molybdenum carbide nanoshoots into nanocomposite electrode
Emre Cevik, Dammam (SA); and Ayhan Bozkurt, Dammam (SA)
Assigned to Imam Abdulrahman Bin Faisal University, Dammam (SA)
Filed by Imam Abdulrahman Bin Faisal University, Dammam (SA)
Filed on Nov. 28, 2023, as Appl. No. 18/520,634.
Application 18/520,634 is a continuation of application No. 18/298,057, filed on Apr. 10, 2023, granted, now 11,869,714.
Application 18/298,057 is a continuation of application No. 17/579,789, filed on Jan. 20, 2022, granted, now 11,682,531, issued on Jun. 20, 2023.
Prior Publication US 2024/0096564 A1, Mar. 21, 2024
This patent is subject to a terminal disclaimer.
Int. Cl. H01G 11/32 (2013.01); H01G 11/62 (2013.01); H01G 11/64 (2013.01); H01G 11/86 (2013.01)
CPC H01G 11/32 (2013.01) [H01G 11/62 (2013.01); H01G 11/64 (2013.01); H01G 11/86 (2013.01)] 12 Claims
OG exemplary drawing
 
1. A method for incorporating nitrogen-doped molybdenum carbide nanosheets into a nanocomposite electrode, comprising:
forming the nitrogen-doped molybdenum carbide nanosheets by:
reacting an ammonium molybdate with an amine substituted heterocycle to form a reaction product; and
thermally treating the reaction product under nitrogen;
mixing at least one binding compound, at least one conductive additive, and at least one electrolyte to form a slurry;
mixing the nitrogen-doped molybdenum carbide nanosheets with the slurry to form a synthesis mixture;
coating the synthesis mixture onto a surface of an electrode substrate; and
drying the nanocomposite electrode at a temperature less than 100° C. to form the nanocomposite electrode;
wherein the nanocomposite electrode comprises:
the electrode substrate;
the nitrogen-doped molybdenum carbide nanosheets;
the at least one electrolyte;
the at least one binding compound; and
the at least one conductive additive;
wherein the electrolyte at least partially penetrates pores of the nitrogen-doped molybdenum carbide nanosheets; and
wherein the nitrogen-doped molybdenum carbide nanosheets are an outer layer of the nanocomposite electrode.