| CPC C01B 3/065 (2013.01) [B01J 21/005 (2013.01); B01J 21/10 (2013.01); B01J 23/22 (2013.01); B01J 35/45 (2024.01); B01J 35/613 (2024.01); B01J 35/633 (2024.01); B01J 35/643 (2024.01); B01J 35/647 (2024.01); B82Y 30/00 (2013.01); B01J 2235/15 (2024.01); C01B 2203/1041 (2013.01); C01B 2203/1205 (2013.01)] | 20 Claims |

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1. A method of hydrogen generation, the method comprising:
contacting sodium borohydride and water in the presence of a catalyst comprising a nanocomposite comprising graphitic C3N4, V2O5, and MgAl2O4 in a mass relationship to each other in a range of from 5 to 15:2 to 7:75 to 95, at a temperature in a range of from 10 to 80° C., thereby catalyzing the hydrogen generation at a hydrogen generation rate in a range of from 2500 to 5000 mL/(min·g).
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