| CPC C25D 11/246 (2013.01) [C23C 22/56 (2013.01); C23C 22/73 (2013.01); C23C 22/83 (2013.01); C23F 11/187 (2013.01)] | 8 Claims |
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1. A sealing process comprising:
impregnating an oxide layer of an anodized metal with a corrosion inhibitor by contacting the oxide layer with a first corrosion inhibitor solution at a first temperature and sealing the impregnated oxide layer of the anodized metal by contacting the impregnated oxide layer with a second corrosion inhibitor solution at a second temperature,
wherein the first corrosion inhibitor solution has a corrosion inhibitor concentration greater than or equal to 1,000 parts per million (ppm) and less than or equal to 15,000 ppm, and the first temperature is less than the second temperature, and the first corrosion inhibitor solution has a pH greater than the second corrosion inhibitor solution;
wherein the second corrosion inhibitor solution has a corrosion inhibitor concentration greater than or equal to 10 ppm and less than or equal to 200 ppm; and
wherein the oxide layer has an interior portion proximate to the metal and an exterior portion distal to the metal and the interior portion includes corrosion inhibitor and the exterior portion includes corrosion inhibitor and oxy-hydroxide compounds of the metal;
wherein the first corrosion inhibitor solution and the second corrosion inhibitor solution comprise chromate or a trivalent chromium compound;
wherein contacting the oxide layer with the first corrosion inhibitor solution occurs for less time than contacting the impregnated oxide layer with the second corrosion inhibitor solution; and
wherein the first temperature is greater than or equal to 10° C. and less than or equal to 60° C.
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