| CPC C30B 1/023 (2013.01) [C01G 39/00 (2013.01)] | 11 Claims |

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1. A composition, comprising:
a population of crystalline transition metal dichalcogenide platelets having the empirical formula MC2, wherein M is a transition metal and C is a chalcogenide,
each of the platelets comprising a region of 3R phase and a region of 2H phase,
each of the platelets being characterized as comprising a single atomic layer to a few atomic layers, and
wherein a majority of the platelets in the population have shapes that are circular, ovoid, American football-shaped, triangular, a 4-sided polygon, a 5-sided polygon, or a 6-sided polygon.
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