US 12,104,127 B2
Method for producing petroleum-based process oils
Mikhail Alekseevich Lazarev, Nizhny Novgorod (RU); and Tatyana Vladimirovna Fedotova, Nizhny Novgorod (RU)
Assigned to ORGKHIM BCH MANAGEMENT COMPANY, JSC, Nizhny Novgorod (RU)
Appl. No. 17/774,343
Filed by ORGKHIM BCH MANAGEMENT COMPANY, JSC, Nizhny Novgorod (RU)
PCT Filed Dec. 27, 2019, PCT No. PCT/RU2019/001032
§ 371(c)(1), (2) Date May 4, 2022,
PCT Pub. No. WO2021/091417, PCT Pub. Date May 14, 2021.
Claims priority of application No. RU2019135648 (RU), filed on Nov. 7, 2019.
Prior Publication US 2022/0363999 A1, Nov. 17, 2022
Int. Cl. C10G 7/00 (2006.01); C08K 5/00 (2006.01); C10G 21/16 (2006.01); C10G 55/06 (2006.01); C10G 61/02 (2006.01)
CPC C10G 7/00 (2013.01) [C08K 5/0016 (2013.01); C10G 21/16 (2013.01); C10G 55/06 (2013.01); C10G 61/02 (2013.01); C10G 2300/1059 (2013.01); C10G 2300/1096 (2013.01); C10G 2300/301 (2013.01); C10G 2300/302 (2013.01); C10G 2300/308 (2013.01); C10G 2400/30 (2013.01)] 1 Claim
 
1. A method for producing a high aromatic non-carcinogenic petroleum-based process oil from by-product fractions of secondary petrochemical processes by fractional distillation, wherein the by-product fractions of secondary petrochemical processes are products of catalytic cracking, or products of catalytic reforming, or aromatic extracts, or mixtures thereof, which have an initial boiling point of no less than 200° C. and a final boiling point of no less than 360° C. at atmospheric pressure and contain no less than 85 wt. % of aromatic constituents, wherein the fractional distillation process is carried out at a reduced or atmospheric pressure and a fractional distillate, which is the high aromatic non-carcinogenic petroleum-based process oil, is withdrawn at temperatures from the initial boiling point to 420° C. in terms of atmospheric pressure, with a reflux ratio of no less than 0.1, wherein the produced high aromatic non-carcinogenic petroleum-based process oil contains no less than 90 wt. % of aromatic constituents, less than 1.0 mg/kg of benzo[a]pyrene and less than 10.0 mg/kg of the sum of the following polycyclic aromatic hydrocarbons (PAHs): benz [a]anthracene; chrysene; benzo[b]fluoranthene; benzo[i]fluoranthene; benzo[k]fluoranthene; benzo[e]pyrene; benzo[a]pyrene; and dibenzo[a,h]anthracene.