| CPC C02F 1/68 (2013.01) [C02F 2101/101 (2013.01)] | 6 Claims |
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1. A polycyclic azide desulfurizer, comprising the following raw materials in parts by mass: 20 parts to 35 parts of an alcohol amine, 20 parts to 35 parts of an amide, and an aldehyde, wherein the aldehyde is 10 parts to 15 parts of a small-molecule aldehyde or 20 parts to 35 parts of a polyaldehyde, wherein the alcohol amine is ethylene glycol amine, and wherein the azide desulfurizer is synthesized by a method comprising the following steps:
1) mixing the alcohol amine with the amide and stirring to obtain a mixture I, heating the mixture I, adding a catalyst I dropwise to the mixture I, and performing reaction to obtain a monocyclic triazine, then heating the monocyclic triazine, mixing with the polyaldehyde and stirring to obtain a mixture II, adding a catalyst II dropwise to the mixture II, and performing coupling reaction while stirring; alternatively,
mixing the small-molecule aldehyde with the amide and stirring to obtain a mixture III, heating the mixture III, adding a catalyst I dropwise to the mixture III, and performing reaction to obtain a reaction system, adding the alcohol amine to the reaction system, adding a catalyst II dropwise thereto, and performing coupling reaction while stirring; and
2) separating a by-product from a product obtained after the coupling reaction out, and purifying the product.
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