US 12,419,335 B2
Readily dissolvable steviol glycoside compositions
Dan S. Gaspard, Victoria, MN (US); and Adam T. Zarth, St. Louis Park, MN (US)
Assigned to CARGILL, INCORPORATED, Wayzata, MN (US)
Filed by CARGILL, INCORPORATED, Wayzata, MN (US)
Filed on Jun. 15, 2023, as Appl. No. 18/335,946.
Application 18/335,946 is a continuation of application No. 16/753,869, abandoned, previously published as PCT/US2018/054698, filed on Oct. 5, 2018.
Claims priority of provisional application 62/676,722, filed on May 25, 2018.
Claims priority of provisional application 62/569,279, filed on Oct. 6, 2017.
Prior Publication US 2024/0082333 A1, Mar. 14, 2024
Int. Cl. A23L 27/30 (2016.01); A23F 3/34 (2006.01); A23L 2/56 (2006.01); A23L 2/60 (2006.01); A23L 2/68 (2006.01); A23L 5/40 (2016.01); A23L 27/00 (2016.01); A61K 31/192 (2006.01); A61K 31/235 (2006.01); A61K 36/28 (2006.01); B01D 15/36 (2006.01); C07H 15/256 (2006.01); C07K 1/16 (2006.01); C07K 1/18 (2006.01)
CPC A23L 27/36 (2016.08) [A23F 3/34 (2013.01); A23L 2/56 (2013.01); A23L 2/60 (2013.01); A23L 2/68 (2013.01); A23L 5/40 (2016.08); A23L 27/30 (2016.08); A23L 27/39 (2016.08); A23L 27/88 (2016.08); A61K 31/192 (2013.01); A61K 31/235 (2013.01); A61K 36/28 (2013.01); B01D 15/361 (2013.01); C07H 15/256 (2013.01); C07K 1/16 (2013.01); C07K 1/18 (2013.01); A23V 2002/00 (2013.01); A23V 2200/15 (2013.01); A23V 2250/258 (2013.01); A61K 2236/31 (2013.01); A61K 2236/39 (2013.01)] 19 Claims
 
1. A method for preparing a steviol glycoside solution, the method comprising:
adding to an aqueous solution crystalline rebaudioside M; one or more dicaffeoylquinic acids or salts thereof; and one or more monocaffeoylquinic acids or salts thereof to form the steviol glycoside solution,
wherein rebaudioside M is at least 70% by weight of total steviol glycosides in the steviol glycoside solution; and
wherein dissolution of rebaudioside M at room temperature is faster than dissolution of rebaudioside M alone without the one or more dicaffeoylquinic acids or salts thereof and without the one or more monocaffeoylquinic acids or salts thereof, such that when the crystalline rebaudioside M; one or more dicaffeoylquinic acids or salts thereof; and one or more monocaffeoylquinic acids or salts thereof added to an aqueous solution to form a 3000 ppm steviol glycoside solution, the rebaudioside M is completely dissolved in less than 15 minutes.