| CPC C25B 11/091 (2021.01) [C25B 11/052 (2021.01); C25B 11/065 (2021.01)] | 13 Claims |

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1. A method of making a metal-N/S-doped carbon electrocatalyst, comprising:
cleaning at least one goat hoof;
sonicating the at least one goat hoof;
calcining the at least one goat hoof at a temperature of 300° C. to produce a carbonaceous precursor;
treating the carbonaceous precursor with a HCl solution;
drying the treated carbonaceous precursor;
adding at least one metal salt to the treated carbonaceous precursor; and
heating the at least one metal salt and the treated carbonaceous precursor to form a metal-N/S-doped carbon electrocatalyst.
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