US 12,409,430 B2
Starch-embedded aroma substance microcapsule and preparation method therefor
Qiang Huang, Guangzhou (CN); Qing Gao, Guangzhou (CN); Bin Zhang, Guangzhou (CN); and Xiong Fu, Guangzhou (CN)
Assigned to SOUTH CHINA UNIVERSITY OF TECHNOLOGY, Guangzhou (CN); and SOUTH CHINA UNIVERSITY OF TECHNOLOGY-ZHUHAI INSTITUTE OF MODERN INDUSTRIAL INNOVATION, Zhuhai (CN)
Filed by SOUTH CHINA UNIVERSITY OF TECHNOLOGY, Guangzhou (CN); and SOUTH CHINA UNIVERSITY OF TECHNOLOGY-ZHUHAI INSTITUTE OF MODERN INDUSTRIAL INNOVATION, Zhuhai (CN)
Filed on Nov. 14, 2022, as Appl. No. 17/986,178.
Application 17/986,178 is a continuation of application No. PCT/CN2021/122770, filed on Oct. 9, 2021.
Claims priority of application No. 202011224511.3 (CN), filed on Nov. 5, 2020.
Prior Publication US 2023/0079081 A1, Mar. 16, 2023
Int. Cl. B01J 13/08 (2006.01); A23L 27/00 (2016.01); B01J 13/20 (2006.01); C08B 30/04 (2006.01); C11B 9/00 (2006.01)
CPC B01J 13/08 (2013.01) [A23L 27/72 (2016.08); B01J 13/206 (2013.01); C08B 30/044 (2013.01); C11B 9/0061 (2013.01); A23V 2002/00 (2013.01)] 10 Claims
 
1. A preparation method for starch-embedded aroma substance microcapsule, characterized in that, it comprises the following steps:
(1) performing degreasing treatment on starch;
(2) high-temperature treatment: dispersing the degreased starch in the step (1) into distilled water to formulate a starch slurry in a range of 5%˜15%, and treating at high temperature of 120˜180° C. for 40˜60 min, then cooling to 50˜100° C. to obtain a starch paste; and
(3) preparation for microcapsule: firstly dispersing an aroma substance with larger molecular cross-sectional area in the starch paste in the step (2), stirring and complexing at 50˜90° C. for 20˜40 min, adding an aroma substance with smaller molecular cross-sectional area, continuing stirring and complexing for 20˜40 min, then naturally cooling, standing still, centrifuging, washing, and drying, to obtain a white powdered product which is the starch-embedded aroma substance microcapsule.