| CPC A61K 36/39 (2013.01) [A61K 9/0073 (2013.01); A61K 9/08 (2013.01); A61K 33/00 (2013.01); A61K 33/06 (2013.01); A61K 36/48 (2013.01); A61K 36/8945 (2013.01); A61K 45/06 (2013.01); A61K 47/02 (2013.01); A61P 11/06 (2018.01); A61P 11/12 (2018.01); A61P 29/00 (2018.01); A61P 37/02 (2018.01); A61P 37/06 (2018.01); A61P 37/08 (2018.01); A61K 2236/00 (2013.01); A61K 2236/15 (2013.01); A61K 2236/17 (2013.01); A61K 2236/37 (2013.01); A61K 2236/53 (2013.01)] | 6 Claims |
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1. A care composition
prepared by the following method:
(1) placing stems and/or a leaves of the sweet potato, a yam-bean, a yam or a combination thereof in a 70-degree Celsius drying oven; and drying until a moisture content is approximately 5-7%, thus preventing organic matters from chelating metallic ions;
(2) placing the dried stems and/or leaves of the sweet potato, the yam-bean, the yam or the combination thereof in a planetary ball mill, and grinding the dried stems and/or leaves to form powder with a particle size of 0.1 μm-1 μm;
(3) pressurizing liquified CO2 to above critical pressure (>72.9 atm) by using a high-pressure pump; the pressurized CO2 is then injected through a heat exchanger, transforming the CO2 to a supercritical fluid; the supercritical fluid is then injected to a high-pressure tank containing the powdered stems and/or leaves of the sweet potato, the yam-bean, the yam or the combination thereof, fat-soluble substances are extracted from the powdered stems and/or leaves of the sweet potato, the yam-bean, the yam or the combination thereof by static extraction for 20 minutes and dynamic extraction for 4 minutes, then reducing the pressure of the high-pressure tank to 1 atm and heating of the high-pressure tank to room temperature, vaporizing the CO2 containing the (extracted) fat soluble substances and then injecting the CO2 containing the (extracted) fat soluble substances into a separating chamber, the CO2 and the fat soluble substances are separated in the separating chamber and the CO2 is then recycled through a chiller;
(4) providing an initial ion solution containing sodium ion, magnesium ion and potassium ion and adjusting the initial ion solution to an isotonic solution through electrodialysis, placing the isotonic solution into a beaker and bringing the isotonic solution to a boil, once boiled, adding in the dried and ground stems and/or leaves of the sweet potato, the yam-bean, the yam or the combination thereof from the step (3) to the boiled isotonic solution; putting a stir-bar into the solution, and covering the beaker with an aluminum foil, stirring for at least an hour at 75-degree Celsius, wherein this process releases mineral ions from the dried and ground stems and/or leaves of the sweet potato, the yam-bean, the yam or the combination thereof, allowing a magnesium ion content in the solution to reach above 0.25% (W/W) and a concentration ratio of magnesium ion to potassium ion to reach 4-17:1 (W/W);
(5) cooling down the solution obtained from the step (4) to room temperature and reducing the sodium ion content in the solution by injecting carbon dioxide to the solution, forming sodium bicarbonate; precipitating the sodium bicarbonate, thus reducing the solution sodium content to less than 0.3% (W/W); and
(6) removing the sodium bicarbonate formed and the residues of the ground stems and/or leaves of the sweet potato, the yam-bean, the yam or a combination thereof, by vacuum filtering the solution through a filter paper (pore size 0.1 μm), wherein the filtered solution is the care composition.
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