US 12,077,556 B2
Process for preparing concentrated solutions of steviol glycosides, and uses
Robert M. Kriegel, Decatur, GA (US); and Indra Prakash, Alpharetta, GA (US)
Assigned to The Coca-Cola Company, Atlanta, GA (US)
Appl. No. 17/056,283
Filed by The Coca-Cola Company, Atlanta, GA (US)
PCT Filed May 17, 2019, PCT No. PCT/US2019/032827
§ 371(c)(1), (2) Date Nov. 17, 2020,
PCT Pub. No. WO2019/222601, PCT Pub. Date Nov. 21, 2019.
Claims priority of provisional application 62/672,799, filed on May 17, 2018.
Prior Publication US 2021/0115081 A1, Apr. 22, 2021
Int. Cl. C07H 15/256 (2006.01); A23L 2/60 (2006.01); A23L 27/30 (2016.01); C07H 1/00 (2006.01)
CPC C07H 15/256 (2013.01) [A23L 2/60 (2013.01); A23L 27/36 (2016.08); C07H 1/00 (2013.01)] 17 Claims
 
1. A method of preparing a concentrated solution having at least about 2 wt % rebaudioside M content comprising:
a. combining (i) a crystalline steviol glycoside composition comprising rebaudioside M, (ii) at least one surfactant selected from a cationic surfactant and an anionic surfactant, and (iii) an aqueous solution to provide a mixture;
b. heating the mixture to provide a clear solution; and
c. cooling the clear solution to about room temperature to provide a concentrate;
wherein the weight ratio of the crystalline steviol glycoside composition comprising rebaudioside M to the at least one surfactant is about 5:1 to about 1:1.