| CPC H01L 21/32136 (2013.01) [H01L 21/32139 (2013.01)] | 15 Claims |

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1. A method of forming a conductive layer of a semiconductor device, comprising:
forming a hard mask layer on a metal layer overlying a substrate, wherein the metal layer comprises tungsten;
patterning the hard mask layer until portions of the metal layer are exposed from the patterned hard mask layer; and
performing a plasma process to the metal layer through the patterned hard mask layer until portions of the substrate are exposed from the etched metal layer, wherein a process gas mixture used in the plasma process comprises a fluorine based gas, a chlorine based gas, and oxygen, wherein the performing the plasma process comprises a first stage and a second stage, the first stage is conducted at a first bias voltage supplied in a first pulse waveform having a first amplitude, the second stage is conducted at a second bias voltage supplied in a second pulse waveform having a second amplitude, the second amplitude is greater than the first amplitude, and the first bias voltage and the second bias voltage are in a range from about 150 V to about 400 V.
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