US 12,391,829 B2
Polyarylene sulfide resin composition, method of preparing polyarylene sulfide resin composition, and heat insulating material manufactured using polyarylene sulfide resin composition
Ran Hee Lee, Daejeon (KR); Soong In Kim, Daejeon (KR); and Myong Jo Ham, Daejeon (KR)
Assigned to LG Chem, Ltd., Seoul (KR)
Appl. No. 17/292,996
Filed by LG CHEM, LTD., Seoul (KR)
PCT Filed Oct. 23, 2020, PCT No. PCT/KR2020/014593
§ 371(c)(1), (2) Date May 11, 2021,
PCT Pub. No. WO2021/080379, PCT Pub. Date Apr. 29, 2021.
Claims priority of application No. 10-2019-0133913 (KR), filed on Oct. 25, 2019; application No. 10-2019-0133914 (KR), filed on Oct. 25, 2019; and application No. 10-2020-0138009 (KR), filed on Oct. 23, 2020.
Prior Publication US 2022/0002544 A1, Jan. 6, 2022
Int. Cl. C08L 81/02 (2006.01); C08K 7/14 (2006.01); C08K 9/06 (2006.01); C08L 79/08 (2006.01)
CPC C08L 81/02 (2013.01) [C08K 7/14 (2013.01); C08K 9/06 (2013.01); C08L 79/085 (2013.01); C08L 2203/20 (2013.01); C08L 2203/30 (2013.01)] 14 Claims
 
1. A polyarylene sulfide resin composition, comprising:
100 parts by weight of a crosslinked polyarylene sulfide having a melt index of 50 to 480 g/10 min;
60 to 120 parts by weight of glass fiber; and
0.1 to 0.3 parts by weight of an anti-hydrolysis agent,
wherein the melt index is measured at 315° C. under a load of 5 kg,
wherein the crosslinked polyarylene sulfide has a polydispersity index (PDI) of 5.4 to 6.4,
wherein the crosslinked polyarylene sulfide contains one or more selected from the group consisting of 2,6-diisopropylphenyl isocyanate, 2,6-diisopropylaniline, 1,4-bis(phenylthio)-benzene, 1,6-hexanediol and p-chloro-N-methylanilin in an amount of 100 ppm or less, and
wherein the polyarylene sulfide resin composition has a volatile weight loss of 0.15% or less at 260° C. for 2 hours.