US 12,018,193 B2
Organic-inorganic hybrid bulk assemblies and methods
Biwu Ma, Tallahassee, FL (US); Chenkun Zhou, Tallahassee, FL (US); Haoran Lin, Tallahassee, FL (US); and Yu Tian, Tallahassee, FL (US)
Assigned to Florida State University Research Foundation, Inc., Tallahassee, FL (US)
Filed by Florida State University Research Foundation, Inc., Tallahassee, FL (US)
Filed on Mar. 8, 2023, as Appl. No. 18/180,601.
Application 18/180,601 is a division of application No. 16/156,218, filed on Oct. 10, 2018, granted, now 11,624,026.
Claims priority of provisional application 62/570,229, filed on Oct. 10, 2017.
Prior Publication US 2023/0383180 A1, Nov. 30, 2023
Int. Cl. C09K 11/06 (2006.01); C09K 11/66 (2006.01); C09K 11/74 (2006.01); C09K 11/77 (2006.01); H05B 33/14 (2006.01); H05B 33/20 (2006.01)
CPC C09K 11/06 (2013.01) [C09K 11/664 (2013.01); C09K 11/7428 (2013.01); C09K 11/7734 (2013.01); H05B 33/145 (2013.01); H05B 33/20 (2013.01); C09K 2211/1007 (2013.01); C09K 2211/1011 (2013.01); C09K 2211/1014 (2013.01); C09K 2211/1018 (2013.01); C09K 2211/1022 (2013.01)] 10 Claims
OG exemplary drawing
 
1. A method of preparing a bulk assembly, the method comprising:
providing a precursor solution comprising—
(i) a solvent;
(ii) one or more compounds of formula M+yXy, wherein M is a metal selected from the group consisting of Sb, Pb, Sn, and Mn; X is Cl, Br, or I; and y is the charge of the metal; and
(iii) one or more organic salts; and
contacting the precursor solution with an anti-solvent to form the bulk assembly.