US 12,013,323 B2
Sample cell for handling and measuring sensitive samples in low temperature conditions
Kok Wai Chan, Espoo (FI); Tianyi Li, Espoo (FI); Juha Hassel, Espoo (FI); and Jari Penttilä, Espoo (FI)
Assigned to IQM Finland Oy, Espoo (FI)
Filed by IQM Finland Oy, Espoo (FI)
Filed on Jun. 29, 2020, as Appl. No. 16/915,644.
Claims priority of application No. 20157942 (EP), filed on Feb. 18, 2020.
Prior Publication US 2021/0255076 A1, Aug. 19, 2021
Int. Cl. G01N 1/42 (2006.01); B08B 9/04 (2006.01); F25D 3/10 (2006.01); H05K 7/20 (2006.01)
CPC G01N 1/42 (2013.01) [B08B 9/04 (2013.01); F25D 3/10 (2013.01); B08B 2209/04 (2013.01); H05K 7/20372 (2013.01)] 20 Claims
OG exemplary drawing
 
1. A sample cell for holding a sample to be placed in a cryogenically cooled environment, the sample cell comprising:
an enclosure adapted to be opened and closed, wherein the enclosure is airtight when closed;
a sample base positioned within the enclosure for receiving the sample;
a refrigerator attachment for attaching the sample cell to a refrigerated body of the cryogenically cooled environment;
a thermal connection between the sample base and the refrigerator attachment;
one or more airtight connectors for establishing electric connections between an inside and an outside of the enclosure;
a conduit extending between the inside and the outside of the enclosure, and through a structure of the enclosure;
a connector positioned at a first end of the conduit adjacent to the outside of the enclosure for connecting an inlet of a vacuum suction pump to the sample cell, the vacuum suction pump used to evacuate the enclosure when the enclosure is closed;
a closing valve for selectively allowing and preventing a flow of gaseous media through the conduit, wherein the closing valve comprises a closing member movable between: (i) an open position in which gaseous media is allowed to flow through the conduit, and (ii) a closed position in which gaseous media is prevented from flowing through the conduit; and
a piece of deformable sealing material compliant with vacuum and cryogenically cooled conditions arranged at a position along the conduit corresponding to a position of the closing valve, such that a portion of the closing member contacts the piece of deformable sealing material when in the closed position to create a seal.