US 12,006,215 B2
Method of carbonizate purification
Marcin Banach, Proszowice (PL); and Jolanta Pullit-Prociak, Michałowice (PL)
Assigned to SYNTOIL SPOLKA AKCYJNA, Wroclaw (PL)
Appl. No. 17/048,589
Filed by SYNTOIL SPÓŁKA AKCYJNA, Wroclaw (PL)
PCT Filed Apr. 15, 2019, PCT No. PCT/IB2019/053077
§ 371(c)(1), (2) Date Oct. 17, 2020,
PCT Pub. No. WO2019/202465, PCT Pub. Date Oct. 24, 2019.
Claims priority of application No. 425261 (PL), filed on Apr. 17, 2018.
Prior Publication US 2021/0155482 A1, May 27, 2021
Int. Cl. C01B 32/05 (2017.01)
CPC C01B 32/05 (2017.08) [C01P 2004/61 (2013.01); C01P 2006/80 (2013.01)] 19 Claims
 
1. A method of purification of carbonizate resulting from the thermal recycling process of rubber waste, characterized in that the carbonizate is mixed with sodium bicarbonate, then deionized water having increased temperature and strong mineral acid and/or mixture of mineral acids are introduced into the obtained mixture, and next the whole is stirred at increased temperature from 70 to 95° C., and filtered at decreased pressure while washing with deionized water having increased temperature, the filtrate is discarded, the solution of a strong base is introduced into the solid residue, and the whole is stirred at increased temperature, then the obtained suspension is filtered at decreased pressure, and washed with deionized water having increased temperature, and next the filtrate is discarded, and the solid residue is dried.