US 11,993,821 B2
Co-crystallized sweeteners
Christopher M. Gregson, Princeton, NJ (US); Matthew P. Sillick, Belle Mead, NJ (US); Jérôme Barra, Geneva (CH); and Angela Di Pietro, Geneva (CH)
Assigned to Firmenich SA, Satigny (CH)
Filed by FIRMENICH SA, Geneva (CH)
Filed on Aug. 6, 2018, as Appl. No. 16/055,266.
Application 16/055,266 is a continuation of application No. 14/654,841, previously published as PCT/EP2013/076635, filed on Dec. 16, 2013.
Claims priority of provisional application 61/745,412, filed on Dec. 21, 2012.
Prior Publication US 2018/0363074 A1, Dec. 20, 2018
Int. Cl. C13B 50/00 (2011.01); A21D 2/18 (2006.01); A23C 9/13 (2006.01); A23C 9/156 (2006.01); A23G 3/36 (2006.01); A23G 4/06 (2006.01); A23L 2/60 (2006.01); A23L 5/00 (2016.01); A23L 27/30 (2016.01); A23L 27/60 (2016.01); A23L 29/30 (2016.01); A23P 10/20 (2016.01); A23P 10/22 (2016.01)
CPC C13B 50/002 (2013.01) [A21D 2/181 (2013.01); A23C 9/1307 (2013.01); A23C 9/156 (2013.01); A23G 3/36 (2013.01); A23G 4/06 (2013.01); A23L 2/60 (2013.01); A23L 5/00 (2016.08); A23L 27/31 (2016.08); A23L 27/33 (2016.08); A23L 27/60 (2016.08); A23L 29/30 (2016.08); A23P 10/20 (2016.08); A23P 10/22 (2016.08); C13B 50/004 (2013.01); A23V 2002/00 (2013.01); A23V 2250/628 (2013.01); A23V 2300/31 (2013.01); A23V 2300/36 (2013.01)] 15 Claims
 
1. A process for forming a co-crystallized composition, wherein the process comprises the steps of:
a. mixing a sugar with water with agitation in the presence of a base to form a sugar composition;
b. heating the sugar composition to evaporate at least a portion of the water and form a sugar syrup;
c. incorporating into the sugar syrup a dry powder of a sweetener to form a uniform dispersion, wherein the sweetener is 3-(4-amino-2,2-dioxide-1H-benzo[c][1,2,6]-thiadiazin-5-yloxy)-2′,2′-dimethyl-N-propylpropanamide;
d. removing the uniform dispersion from the heat; and
e. allowing the uniform dispersion to cool with vigorous agitation to form a co-crystallized composition comprising the sugar and the sweetener.