US 11,987,712 B2
Carbon black generating system
Ned J. Hardman, Woodside, CA (US); Roscoe W. Taylor, San Mateo, CA (US); Robert J. Hanson, San Carlos, CA (US); and Peter L. Johnson, Mountain View, CA (US)
Assigned to MONOLITH MATERIALS, INC., Redwood City, CA (US)
Appl. No. 15/548,346
Filed by MONOLITH MATERIALS, INC., Redwood City, CA (US)
PCT Filed Feb. 1, 2016, PCT No. PCT/US2016/015941
§ 371(c)(1), (2) Date Aug. 2, 2017,
PCT Pub. No. WO2016/126599, PCT Pub. Date Aug. 11, 2016.
Claims priority of provisional application 62/111,346, filed on Feb. 3, 2015.
Prior Publication US 2018/0022925 A1, Jan. 25, 2018
Int. Cl. C09C 1/48 (2006.01); B01J 19/08 (2006.01)
CPC C09C 1/485 (2013.01) [B01J 19/088 (2013.01); B01J 2219/0809 (2013.01); B01J 2219/0869 (2013.01); B01J 2219/0871 (2013.01); B01J 2219/0875 (2013.01); B01J 2219/0898 (2013.01); C01P 2006/12 (2013.01); C01P 2006/19 (2013.01)] 34 Claims
 
1. A method of making carbon black particles in an enclosed particle generating reactor, comprising:
generating a plasma comprising at least 60% by volume hydrogen with plasma generating electrodes in a reactor, wherein an interior dimension of the reactor is at least 10% smaller downstream of the plasma generating electrodes;
injecting, through injectors, hydrocarbon either at a point where the interior dimension is smallest or further downstream from the plasma generating electrodes to form carbon black particles comprising a first amount of a combustible gas, wherein a sum of diameters of the injectors is greater than 5% of a circumference of a cross-sectional plane of the reactor where the injectors are co-located; and
reducing the combustible gas present in the carbon black particles such that the carbon black particles comprise a second amount of the combustible gas after said reducing, wherein the second amount is less than 10% of the first amount.