US 12,305,120 B2
Lotus leaf derived biochar loaded with ZIF-67, and preparation method therefor and application method thereof
Hongyou Wan, Zhengzhou (CN); Jingwei Yan, Zhengzhou (CN); Wei Zhang, Zhengzhou (CN); Lin Gong, Zhengzhou (CN); Xinfeng Zhu, Zhengzhou (CN); Chaohai Wang, Zhengzhou (CN); and Cong Guo, Zhengzhou (CN)
Assigned to Zhengzhou University, Zhengzhou (CN)
Filed by Zhengzhou University, Zhengzhou (CN)
Filed on Jul. 26, 2023, as Appl. No. 18/358,957.
Claims priority of application No. 202210963341.3 (CN), filed on Aug. 11, 2022.
Prior Publication US 2024/0052245 A1, Feb. 15, 2024
Int. Cl. C10B 53/02 (2006.01)
CPC C10B 53/02 (2013.01) 8 Claims
OG exemplary drawing
 
1. A preparation method of lotus leaf derived biochar loaded with zeolite-imidazolate framework-67 (ZIF-67), comprising:
drying a lotus leaf at a temperature of 50-90 Celsius degree (° C.) for 1-5 hours (h) to remove moisture therein to thus obtain a dried lotus leaf, and cutting the dried lotus leaf to obtain a pretreated lotus leaf carrier; and
adding the pretreated lotus leaf carrier and ZIF-67 to methanol as solvent, to obtain a solution, performing an ultrasonic dispersion process on the solution, standing the solution after performing the ultrasonic dispersion process to perform a self-assembly reaction to thus obtain a reacted solution, and drying the reacted solution to obtain the lotus leaf derived biochar loaded with the ZIF-67, wherein a drying temperature for drying the reacted solution is 200-220° C., and a drying time for drying the reacted solution is 4-9 h.