US 11,959,022 B2
Extruder systems and processes for production of petroleum coke and mesophase pitch
Hasan Ali Al-Hashmy, Dhahran (SA); and Ibrahim Al-Nutaifi, Dhahran (SA)
Assigned to Saudi Arabian Oil Company, Dhahran (SA)
Filed by Saudi Arabian Oil Company, Dhahran (SA)
Filed on Nov. 23, 2021, as Appl. No. 17/534,178.
Prior Publication US 2023/0159828 A1, May 25, 2023
This patent is subject to a terminal disclaimer.
Int. Cl. C10B 31/06 (2006.01); C10B 37/04 (2006.01); C10B 57/00 (2006.01); C10B 57/04 (2006.01); D01F 9/155 (2006.01); D01F 9/32 (2006.01)
CPC C10B 31/06 (2013.01) [C10B 37/04 (2013.01); C10B 57/005 (2013.01); C10B 57/04 (2013.01); D01F 9/155 (2013.01); D01F 9/322 (2013.01)] 11 Claims
OG exemplary drawing
 
1. A method of production for consistently sized and shaped optically anisotropic mesophase pitch from vacuum residue, the method comprising the steps of:
fractionating vacuum residue, produced in a vacuum distillation column at a temperature between about 430° C. to about 450° C. and a pressure of about 0.1 kPa, to remove liquid propane gas, fuel gas, coker naphtha, light coker gas oil, and heavy coker gas oil to produce a processed vacuum reside;
supplying the processed vacuum residue to an extruder;
heating the processed vacuum residue throughout a horizontal profile of the extruder from an inlet to an outlet of the extruder, wherein temperature of the extruder at the inlet is about 550° F. and decreases gradually along the horizontal profile to the outlet of the extruder to between about 50° F. and about 350° F., wherein pressure along the horizontal profile of the extruder is between about 0.1 kPa and 1 kPa;
venting hydrocarbon off-gases from the extruder along the horizontal profile of the extruder from the inlet to the outlet of the extruder; and
physically shaping the consistently sized and shaped mesophase pitch at the outlet of the extruder for production of carbon fibers.