| CPC B32B 9/047 (2013.01) [B32B 7/12 (2013.01); B32B 33/00 (2013.01); B32B 37/10 (2013.01); B32B 2262/106 (2013.01); B32B 2264/1021 (2020.08); B32B 2264/107 (2013.01); B32B 2264/303 (2020.08); B32B 2305/08 (2013.01); B32B 2305/22 (2013.01); B32B 2305/30 (2013.01); B32B 2307/304 (2013.01); B32B 2307/3065 (2013.01); B32B 2307/72 (2013.01)] | 4 Claims |
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1. A nano-silica composite thermal insulation material, comprising a reinforcement mesh and thermal insulation layers arranged on two sides of the reinforcement mesh, the reinforcement mesh and the thermal insulation layers are bonded by an inorganic binder; wherein
raw materials of each of the thermal insulation layers comprises the following components in parts by weight: 60-90 parts of nano-silica, 15-35 parts of a light-screening agent and 1-10 parts of a fiber;
the light-screening agent is silicon carbide with a particle size of 0.01-15 μm;
the fiber comprises a glass fiber, a high-silica fiber and a carbon fiber in a weight ratio of (1-2):(2-3):1; a diameter of the fiber is 3-15 μm and a length of the fiber is 10-20 mm;
the nano-silica is fumed silica or silica aerogel;
a bulk density of the fumed silica is 20-100 g/m3;
the carbon fiber is coated with a polyamide acid coating on a surface of the carbon fiber, and the carbon fiber coated with the polyamide acid coating is prepared by: dissolving pyromellitic dianhydride and diaminodiphenyl ether in N,N-dimethylamide for reaction in a presence of nitrogen, then adjusting a value of pH to 9 with ammonia water to obtain a mixing solution, impregnating the carbon fiber with the mixing solution, and then drying and dispersing the carbon fiber to obtain the carbon fiber coated with the polyamide acid coating;
the reinforcement mesh is a glass fiber mesh, a high-silica fiber mesh, a basalt fiber mesh, a ceramic fiber mesh, a pre-oxidized fiber mesh, a carbon fiber mesh, or a metal mesh;
a method for preparing the nano-silica composite thermal insulation material comprises the following steps:
weighing the raw materials of the thermal insulation layers and mixing the raw materials;
laying a first layer of the raw materials of the thermal insulation layers, spraying the inorganic binder on the first layer of the raw materials of the thermal insulation layers, laying the reinforcement mesh on the first layer of the raw materials of the thermal insulation layers, spraying the inorganic binder on the reinforcement mesh, and then laying a second layer of the raw materials of the thermal insulation layers on the reinforcement mesh to obtain a semi-finished product; and
pressing the semi-finished product with a pressure of 0.001-0.2 MPa firstly, and then increasing the pressure to 1-5 MPa at a rate of 0.1-0.3 MPa/min for pressing and molding, thus obtaining the nano-silica composite thermal insulation material.
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