US 12,264,412 B2
Process for manufacturing lyocell filament yarn and an apparatus thereof
Lalaso Vishnu Mohite, Maharashtra (IN); Shailesh Prakash Nagarkar, Maharashtra (IN); Santosh Shivaji Shingote, Maharashtra (IN); Shirish Sheshrao Thakre, Maharashtra (IN); Suvankar Madhusudan Dutta, Maharashtra (IN); Bandu Madhukar Kale, Gujarat (IN); Roop Kishore Sharma, Gujarat (IN); Manishkumar Govindbhai Limbani, Gujarat (IN); Srivastava Pankaj, Girsomnath (IN); and Harendra Singh Dagur, Gujarat (IN)
Assigned to ADITYA BIRLA SCIENCE AND TECHNOLOGY COMPANY PVT. LTD., Maharashtra (IN); and GRASIM INDUSTRIES LTD., Madhya Pradesh (IN)
Appl. No. 17/607,987
Filed by Aditya Birla Science and Technology Company Pvt. Ltd., Maharashtra (IN); and Grasim Industries Ltd., Madhya Pradesh (IN)
PCT Filed Apr. 30, 2020, PCT No. PCT/IN2020/050395
§ 371(c)(1), (2) Date Nov. 1, 2021,
PCT Pub. No. WO2020/222258, PCT Pub. Date Nov. 5, 2020.
Claims priority of application No. 201921012927 (IN), filed on Apr. 30, 2019.
Prior Publication US 2022/0290329 A1, Sep. 15, 2022
Int. Cl. D01D 5/00 (2006.01); D01D 5/06 (2006.01); D01D 10/00 (2006.01); D01D 10/06 (2006.01); D01F 2/00 (2006.01); D02J 1/00 (2006.01); D02J 1/22 (2006.01)
CPC D01D 5/06 (2013.01) [D01D 10/06 (2013.01); D01F 2/00 (2013.01); D02J 1/223 (2013.01)] 11 Claims
OG exemplary drawing
 
1. An apparatus for manufacturing lyocell filament yarn with improved mechanical properties, the apparatus comprising:
a) at least one lyocell dope vessel for storing cellulose dope;
b) at least one metering pump for pumping said cellulose dope into at least one spin pack containing at least one spinneret that extrudes the cellulose dope as spun filament yarn;
c) a regeneration bath containing a solution for partial regeneration of the extruded spun filament yarn;
d) at least one winder for stretching extruded spun filament yarn while it passes through an air-gap of controlled conditions and the regeneration bath solution to create a stretched yarn;
e) an individual yarn guiding drum;
f) a main drum having a filament yarn washing section and a filament yarn drying section,
wherein the individual yarn guiding drum guides the stretched yarn from the at least one winder to the main drum spinning at a speed less than the winder speed, wherein the main drum speed to winder speed is selected from a ratio of 1.00 to 0.85, wherein the filament yarn washing section comprises sequential washing zones, each successive washing zone containing a washing solution of successively decreasing concentration of N-methyl morpholine N-oxide (NMMO), said concentration successively decreasing to up to 0% by weight of NMMO, and
wherein the filament yarn drying section has a temperature of 40° C. to 100° C. for drying the washed filament yarn to create a dried lyocell filament yarn having a tenacity greater than 3.2 grams per denier and elongation greater than 8%; and
g) a circulating pump to maintain uniform concentration of the NMMO in each washing zone.