US 12,264,222 B2
Method for preparation of antibacterial bio-filler for plastic and antibacterial bio-filler for plastic prepared thereby
Sang-Hyun Lee, Daejeon (KR)
Assigned to LIGNUM INC., Daejeon (KR)
Appl. No. 17/634,168
Filed by LIGNUM Inc., Daejeon (KR)
PCT Filed Oct. 28, 2020, PCT No. PCT/KR2020/014836
§ 371(c)(1), (2) Date Feb. 9, 2022,
PCT Pub. No. WO2022/092343, PCT Pub. Date May 5, 2022.
Prior Publication US 2022/0356308 A1, Nov. 10, 2022
Int. Cl. C08H 8/00 (2010.01); C08J 3/14 (2006.01); C08J 3/20 (2006.01); C08L 1/02 (2006.01); C08L 97/02 (2006.01)
CPC C08H 8/00 (2013.01) [C08J 3/14 (2013.01); C08J 3/20 (2013.01); C08L 1/02 (2013.01); C08L 97/02 (2013.01)] 11 Claims
OG exemplary drawing
 
1. A method for preparing a bio-filler for a plastic, the method comprising the steps of:
(a) removing at least a part of hemicellulose from lignocellulosic biomass to form hemicellulose-removed lignocellulosic biomass, wherein the lignocellulosic biomass comprises lignin, cellulose, and hemicellulose;
(b) modifying the hemicellulose-removed lignocellulosic biomass with an acid to form an acid-treated reaction mixture; and
(c) adding a base to the acid-treated reaction mixture to neutralize remaining acidic components to form a neutralized reaction mixture, followed by removing water-soluble materials from the neutralized reaction mixture to form solid particles,
wherein the solid particles obtained in step (c) contain hemicellulose-derived components formed through step (b) and step (c) in an amount of 3 wt % or less, based on the total weight of lignin-derived components, cellulose-derived components, and hemicellulose-derived components formed through step (b) and step (c).