US 12,258,544 B2
Process for making a particulate laundry detergent composition
Joss Prest, Newcastle upon Tyne (GB); Zoe Dyter, Newcastle upon Tyne (GB); Eric San Jose Robles, Newcastle upon Tyne (GB); and Hossam Hassan Tantawy, Northumberland (GB)
Assigned to The Procter & Gamble Company, Cincinnati, OH (US)
Filed by The Procter & Gamble Company, Cincinnati, OH (US)
Filed on Jan. 5, 2023, as Appl. No. 18/093,629.
Application 18/093,629 is a continuation of application No. PCT/US2021/040221, filed on Jul. 2, 2021.
Claims priority of application No. 20184329 (EP), filed on Jul. 6, 2020.
Prior Publication US 2023/0145083 A1, May 11, 2023
Int. Cl. C11D 11/00 (2006.01); C11D 1/22 (2006.01); C11D 1/83 (2006.01); C11D 3/20 (2006.01); C11D 3/22 (2006.01); C11D 3/50 (2006.01); C11D 11/02 (2006.01); C11D 17/06 (2006.01); C11D 1/29 (2006.01)
CPC C11D 3/505 (2013.01) [C11D 1/83 (2013.01); C11D 3/2086 (2013.01); C11D 3/226 (2013.01); C11D 11/02 (2013.01); C11D 17/06 (2013.01); C11D 1/22 (2013.01); C11D 1/29 (2013.01); C11D 2111/12 (2024.01)] 15 Claims
 
1. A process for making a particulate laundry detergent composition, wherein the process comprises the steps of:
(a) contacting water, starch, acid and perfume to form a concentrated acidic mixture, wherein the concentrated acidic mixture comprises:
(i) from about 20 wt % to about 60 wt % starch;
(ii) from about 10 wt % to about 50 wt % perfume;
(ii) from about 2 wt % to about 20 wt % acid;
(iv) from about 10 wt % to less than about 45 wt % water; and
wherein the concentrated acidic mixture has a pH of less than about 4.5;
(b) subjecting the concentrated acidic mixture to a perfume emulsification step to emulsify the perfume to form an emulsified perfume mixture in fluid form; and
(c) spraying the emulsified perfume mixture in fluid form onto base detergent particles so that the emulsified perfume mixture at least partially coats the base detergent particles to form the particulate laundry detergent composition, wherein the base detergent particles comprise from about 4 wt % to about 60 wt % detersive surfactant.