US 12,252,413 B1
Preparation method for ultra-high compacted lithium iron phosphate cathode material and lithium battery
Xinlong Huang, Xiangtan (CN); Tao Chen, Xiangtan (CN); Kun Cheng, Xiangtan (CN); and Yang Yu, Xiangtan (CN)
Assigned to Hunan Yuneng new energy battery materials Co., LTD., Hunan (CN)
Filed by Hunan Yuneng new energy battery materials Co., LTD., Xiangtan (CN)
Filed on Dec. 3, 2024, as Appl. No. 18/967,417.
Claims priority of application No. 202410819387.7 (CN), filed on Jun. 24, 2024.
Int. Cl. C01G 49/00 (2006.01); H01M 10/052 (2010.01)
CPC C01G 49/009 (2013.01) [H01M 10/052 (2013.01); C01P 2004/03 (2013.01); C01P 2006/40 (2013.01)] 4 Claims
OG exemplary drawing
 
1. A preparation method for ultra-high compacted lithium iron phosphate cathode material, comprising: S1. conducting a chemical reaction based on iron phosphate and dispersant to obtain an iron-containing precursor; S2. obtaining an iron-containing precursor mixture by mixing the iron-containing precursor, a borane, a lithium source, a phosphorus source, and a first carbon source; using ultraviolet light to irradiate the iron-containing precursor mixture; performing a first sintering to the irradiated iron-containing precursor mixture and crushing to obtain a first precursor mixture, grinding the first precursor mixture to a first preset particle size to obtain a first precursor, wherein the borane is a borane nanosheet or a borane nanomembrane; S3. mixing and grinding the iron-containing precursor, the lithium source, the phosphorus source, and a second carbon source, performing a second sintering to obtain a second precursor mixture, and grinding the second precursor mixture to a second preset particle size to obtain a second precursor, where the second carbon source is an amino acid chelated titanium; S4. mixing the first precursor, the second precursor, and a third carbon source, then drying and performing a third sintering in an inert gas atmosphere to obtain the lithium iron phosphate cathode material.