US 12,251,408 B2
Postbiotic preparation for pelvic floor muscle rehabilitation and preparation method and application thereof
Yuan Xu, Jinan (CN)
Assigned to SHANDONG NICE HEALTH TECHNOLOGY CO., LTD., Jinan (CN)
Filed by SHANDONG NICE HEALTH TECHNOLOGY CO., LTD., Shandong (CN)
Filed on Jan. 10, 2024, as Appl. No. 18/408,667.
Claims priority of application No. 202310502907.7 (CN), filed on May 6, 2023.
Prior Publication US 2024/0366692 A1, Nov. 7, 2024
Int. Cl. A61K 35/747 (2015.01); A61K 9/00 (2006.01); A61P 21/00 (2006.01); C12N 1/20 (2006.01); C12R 1/25 (2006.01)
CPC A61K 35/747 (2013.01) [A61K 9/0053 (2013.01); A61P 21/00 (2018.01); C12N 1/205 (2021.05); C12R 2001/25 (2021.05)] 11 Claims
 
1. A microbial agent, comprising an inactivated strain of L. plantarum Nice-02, preserved in CCTCC (China Center for Type Culture Collection) on Apr. 21, 2023 with a biological preservation number of CCTCC NO: M 2023571;
wherein the microbial agent is prepared by a method comprising:
S1: activation culture: performing plate streaking on the L. plantarum Nice-02 into an activation culture medium to obtain a pure strain;
S2: primary seed solution preparation: picking and placing a single colony of the L. plantarum Nice-02 prepared in S1 into a first culture solution at 28 to 30° C. for stationary culture for 12 to 14 h to obtain a primary seed solution;
S3: secondary seed solution preparation: inoculating the primary seed solution into a second culture solution according to an inoculation amount of 0.1 to 5% for stationary culture at 30° C. to 40° C. for 10 to 12 h to obtain a secondary seed solution;
S4: tertiary seed solution preparation: inoculating the cultured secondary seed solution into a seeding tank containing a third culture solution under an aseptic condition at an inoculation amount of 0.5 to 5%, and performing stir culture at a stirring speed of 20 to 50 r/min, a temperature of 30° C. to 40° C., a pH value of 7.0 and a tank pressure of 0.03 to 0.06 MPa to obtain a tertiary seed solution after the culture for 10 to 12 h;
S5: L. Plantarum primary fermentation: inoculating the tertiary seed solution into a fermentation tank containing a sterilized culture solution at an inoculation amount of 0.5 to 5%, a temperature of 32° C., a stirring speed of 40 to 50 r/min to be cultured for 5 to 6 h;
S6: L. plantarum secondary fermentation: after 5 to 6 h, lowering the fermentation temperature to 30° C., accelerating the stirring speed to 50 to 70 r/min, keeping the tank pressure at 0.05 MPa and the natural pH, and performing fermentation for 3 to 4 h;
S7: L. plantarum tertiary fermentation: after 8 to 10 h, keeping the stirring speed unchanged, raising the fermentation temperature to 35° C., keeping the tank pressure at 0.05 MPa, keeping the pH value at 6.5, and performing fermentation for 2 h;
S8: L. plantarum quaternary fermentation: after 10 to 12 h, decelerating the stirring speed to 30 to 40 r/min, raising the fermentation temperature to 40° C., keeping the tank pressure at 0.05 MPa and the pH value at 6.5, and performing fermentation for 1 to 2 h to obtain a fermentation solution; and
S9: L. plantarum quinary fermentation: after 11 to 14 h, keeping the stirring speed unchanged, raising the temperature to 45° C., adding sterile lipoteichoic acid accounting for 0.05 to 0.2% of the volume of the fermentation solution into the fermentation tank, lowering the temperature to 20° C., and keeping the state for 30 min;
wherein the microbial agent is obtained by performing high-temperature inactivation and spray drying the fermentation solution prepared in S9.