US 12,247,157 B2
Biologically derived cement retarder
James Robert Benkley, Duncan, OK (US); Ronnie G. Morgan, Waurika, OK (US); and Thomas Jason Pisklak, Houston, TX (US)
Assigned to Halliburton Energy Services, Inc., Houston, TX (US)
Filed by Halliburton Energy Services, Inc., Houston, TX (US)
Filed on Jul. 15, 2022, as Appl. No. 17/866,311.
Prior Publication US 2024/0018409 A1, Jan. 18, 2024
Int. Cl. C09K 8/467 (2006.01)
CPC C09K 8/467 (2013.01) 8 Claims
OG exemplary drawing
 
1. A method for cementing in a subterranean formation, comprising:
obtaining pulp waste residue from a sweetener manufacturing process; wherein the source of a sweetener for the sweetener manufacturing process is sugar cane, beet, citrus, maize, grain sorghum, pineapple, and any combination thereof;
processing the pulp waste residue by washing the pulp waste residue with a liquid or steam, then extracting the liquid effluent from the washed pulp waste residue, then drying the extracted liquid effluent to produce a dried extract, and then grinding and/or sieving the dried extract to produce the cement retarder; wherein the cement retarder comprises a sugar concentration of at least 40%, a Brix value of at least 60, a nitrogen-free extract concentration of at least 50%, a total solids concentration of at least 60%, a crude protein concentration less than 10%, a fat concentration less than 5%, a fiber concentration less than 5%, and an ash concentration less than 10%;
providing a cement composition comprising an aqueous fluid, a cement, and the cement retarder;
introducing the cement composition into a wellbore penetrating a subterranean formation;
pumping the cement composition to a location within the wellbore; and
allowing the cement composition to set in the location.