CPC B01J 29/7815 (2013.01) [B01J 21/04 (2013.01); B01J 29/084 (2013.01); B01J 29/80 (2013.01); B01J 35/615 (2024.01); B01J 35/633 (2024.01); B01J 35/635 (2024.01); B01J 35/647 (2024.01); B01J 37/0018 (2013.01); B01J 37/031 (2013.01); B01J 37/04 (2013.01); B01J 37/08 (2013.01); C10G 47/20 (2013.01); B01J 2029/062 (2013.01); C10G 2300/202 (2013.01); C10G 2300/301 (2013.01); C10G 2300/308 (2013.01)] | 20 Claims |
1. A method for producing a catalyst composition, the method comprising:
forming a precursor solution comprising a silicon-containing material, an aluminum-containing material, and a quaternary amine;
hydrothermally treating the precursor solution at a first temperature to form an intermediate mixture;
hydrothermally treating the intermediate mixture at a second temperature to form beta zeolite, wherein the first temperature is less than the second temperature by at least 200° C.;
forming an extrudable mixture comprising the beta zeolite, alumina, a metal precursor, and a binder;
extruding the extrudable mixture to form extrudates; and
calcining the extrudates to form the catalyst composition.
|