US 11,913,935 B2
Method for evaluating properties of polypropylene resin, method for preparing polypropylene non-woven fabric, and polypropylene non-woven fabric
Hyunsup Lee, Daejeon (KR); Seong Min Chae, Daejeon (KR); Kyung Seop Noh, Daejeon (KR); Heekwang Park, Daejeon (KR); Ki Soo Lee, Daejeon (KR); Sangjin Jeon, Daejeon (KR); and Myunghan Lee, Daejeon (KR)
Assigned to LG Chem, Ltd., (KR)
Appl. No. 17/059,724
Filed by LG Chem, Ltd., Seoul (KR)
PCT Filed Jun. 21, 2019, PCT No. PCT/KR2019/007542
§ 371(c)(1), (2) Date Nov. 30, 2020,
PCT Pub. No. WO2019/245338, PCT Pub. Date Dec. 26, 2019.
Claims priority of application No. 10-2018-0072318 (KR), filed on Jun. 22, 2018.
Prior Publication US 2021/0215661 A1, Jul. 15, 2021
Int. Cl. G01N 33/36 (2006.01); D04H 1/4291 (2012.01); D04H 1/56 (2006.01); D04H 3/007 (2012.01)
CPC G01N 33/367 (2013.01) [D04H 1/4291 (2013.01); D04H 1/565 (2013.01); D04H 3/007 (2013.01); G01N 2203/0075 (2013.01)] 13 Claims
 
1. A method for evaluating a loft property of a propylene non-woven fabric prepared by a melt blown process of a combination of a first polypropylene resin and a second polypropylene resin, the method comprising steps of:
preparing a first sample of the first polypropylene resin and preparing a second sample of the second polypropylene resin, respectively;
deriving a residual stress ratio of the first sample and a residual stress ratio of the second sample, respectively, by the steps of:
applying 150 to 250% strain to each sample;
a first time (Time S1) after applying the strain, measuring a first residual stress (Stress S1);
a second time (Time S2) after applying the strain, measuring a second residual stress (Stress S2); and
deriving a residual stress ratio represented by Equation 1:
Residual stress ratio=Stress S2/Stress S1  [Equation 1]
in Equation 1,
Stress S1 is the first residual stress measured after the first time (Time S1),
Stress S2 is the second residual stress measured after the second time (Time S2), and
Time S2>Time S1,
comparing the residual stress ratio of the first sample and the residual stress ratio of the second sample, and
determining that the loft property of the propylene non-woven fabric is appropriate if the residual stress ratio of the first sample is at least 10 times the residual stress ratio of the second sample.