CPC C09C 1/3081 (2013.01) [B01D 45/16 (2013.01); B01D 46/02 (2013.01); B01D 50/20 (2022.01); C09C 3/12 (2013.01); B01J 8/18 (2013.01); B01J 8/24 (2013.01); B01J 8/26 (2013.01); B05D 1/22 (2013.01)] | 13 Claims |
1. A combined treatment method for surface modification of fumed silica, comprising the following steps:
step (1) two sets of modification devices are used to jointly treat fumed silica, each of which includes a reaction furnace and a gas separator; the fumed silica is treated with a modifier in the reaction furnace of each set of modification devices, and two groups of modified fumed silica and exhaust gas are obtained respectively;
step (2) the exhaust gas obtained in the step (1) is separated respectively to obtain unreacted modifier and by-products; and the obtained by-products are input into the reaction furnace of the other set of modification devices as reaction assistants to participate in the modification reaction; and the obtained unreacted modifiers are returned to the reaction furnace of the original modification devices for repeated use;
wherein, the modifiers used in the two sets of modification devices are different from each other and are selected from organochlorosilanes, alkylsiloxanes, alkylsilazanes, hydroxyl-terminated polysiloxanes and cyclosiloxanes; wherein, the modifiers used in the two sets of modification devices are not both selected from hydroxyl-terminated polysiloxanes or cyclosiloxanes.
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