US 12,227,599 B2
Preparation method of PVA fiber
Jianguo Lu, Shaoxing (CN)
Assigned to Zhende Medical Co., Ltd., Shaoxing (CN)
Filed by Zhende Medical Co., Ltd., Shaoxing (CN)
Filed on Mar. 29, 2021, as Appl. No. 17/215,338.
Application 17/215,338 is a continuation of application No. PCT/CN2019/110559, filed on Oct. 11, 2019.
Prior Publication US 2021/0214475 A1, Jul. 15, 2021
Int. Cl. C08F 116/06 (2006.01)
CPC C08F 116/06 (2013.01) 9 Claims
OG exemplary drawing
 
1. A preparation method of polyvinyl alcohol (PVA) fiber comprising the following steps:
step 1, preparing a spinning dope;
PVAc is used as a raw material, and dissolved with addition of methanol before filtration, and then the spinning dope is obtained;
step 2, spinning;
the spinning dope is injected into a spinneret, and the ejected fibers are brought into a direct current electrolytic cell, the PVAc undergoing a series of reactions of an alcoholysis, an electrolytic catalytic alcoholysis, and a levering of the alcohol; the solution formulation in an electrolytic coagulation bath comprising alkali, alcohol, and water;
step 3: acid bath;
the fiber passing through the electrolytic cell is placed into an acid solution with pH value of 4.5-6.9 for an acid bath;
step 4: forming a finished polyvinyl alcohol fiber product by stretching, drying, washing with water, crimping with hot water and packaging.