US 12,221,345 B2
Process for the preparation of a porous carbonaceous material, porous carbonaceous material, and a catalyst made of the material
Markus Klose, Hanau (DE); Stephan Osinga, Hanau (DE); Julie Michaud-Bernlochner, Hanau (DE); Dominik Samuelis, Hanau (DE); Jörg Becker, Hanau (DE); Thomas Hucke, Hanau (DE); Benjamin Krüner, Hanau (DE); and Evgeniia Komarova, Hanau (DE)
Assigned to HERAEUS BATTERY TECHNOLOGY GMBH, Hanau (DE)
Appl. No. 17/436,854
Filed by Heraeus Battery Technology GmbH, Hanau (DE)
PCT Filed Mar. 19, 2020, PCT No. PCT/EP2020/057622
§ 371(c)(1), (2) Date Sep. 7, 2021,
PCT Pub. No. WO2020/200812, PCT Pub. Date Oct. 8, 2020.
Claims priority of application No. 19166727 (EP), filed on Apr. 2, 2019.
Prior Publication US 2022/0177309 A1, Jun. 9, 2022
Int. Cl. C01B 32/05 (2017.01)
CPC C01B 32/05 (2017.08) [C01P 2004/64 (2013.01); C01P 2006/10 (2013.01); C01P 2006/14 (2013.01); C01P 2006/16 (2013.01)] 19 Claims
 
1. A process for the preparation of a porous carbonaceous material comprising:
a) providing at least one carbon source and at least one amphiphilic species,
b) combining at least the carbon source and the amphiphilic species to obtain a precursor material,
c) heating the precursor material to a temperature in the range between 350° C. and 550° C. for at least 15 min so as to obtain the porous carbonaceous material, and
d) cooling the porous carbonaceous material having a modal pore size and a pore volume and a skeleton density
e) comminuting the porous carbonaceous material so as to obtain crushed porous carbonaceous material particles, and
f) heating the crushed porous carbonaceous material particles to a temperature in the range from 700-1500° C.