	US 11,873,273 B2
	Online production of organic peroxide using a catalyst bed
Todd Coleman, Batesville, AR (US); Tim Yeaman, Russellville, AR (US); and Slaton Fry, Conway, AR (US)
Assigned to SAFE FOODS CORPORATION, North Little Rock, AR (US)
Appl. No. 16/981,666
Filed by SAFE FOODS CORPORATION, North Little Rock, AR (US)
PCT Filed Mar. 28, 2019, PCT No. PCT/US2019/024516 § 371(c)(1), (2) Date Sep. 16, 2020, PCT Pub. No. WO2019/191387, PCT Pub. Date Oct. 3, 2019.
Claims priority of provisional application 62/649,988, filed on Mar. 29, 2018.
Prior Publication US 2021/0009515 A1, Jan. 14, 2021
Int. Cl. C07C 407/00 (2006.01); B01J 4/00 (2006.01); B01J 8/00 (2006.01); B01J 8/02 (2006.01)

CPC C07C 407/00 (2013.01) [B01J 4/008 (2013.01); B01J 8/001 (2013.01); B01J 8/0278 (2013.01); B01J 2204/005 (2013.01); B01J 2208/00628 (2013.01); B01J 2208/00823 (2013.01); B01J 2208/00964 (2013.01)]

9 Claims

1. A method of producing an organic peroxide comprising:

introducing an organic solution and a peroxide solution into a mixing tank to form a mixture;

circulating the mixture over a fixed catalyst bed to form the organic peroxide;

measuring a concentration of the organic peroxide in the mixture; and

removing at least a portion of the mixture when the concentration reaches a set value.