US 11,866,325 B2
Synthesis of mordenite using multiple organics
Jeffrey D. Rimer, Houston, TX (US); and Manjesh Kumar, Houston, TX (US)
Assigned to UNIVERSITY OF HOUSTON SYSTEM, Houston, TX (US)
Appl. No. 17/054,861
Filed by University of Houston System, Houston, TX (US)
PCT Filed May 15, 2019, PCT No. PCT/US2019/032450
§ 371(c)(1), (2) Date Nov. 12, 2020,
PCT Pub. No. WO2019/222371, PCT Pub. Date Nov. 21, 2019.
Claims priority of provisional application 62/672,291, filed on May 16, 2018.
Prior Publication US 2021/0214237 A1, Jul. 15, 2021
Int. Cl. C01B 39/26 (2006.01)
CPC C01B 39/265 (2013.01) [C01P 2002/01 (2013.01); C01P 2002/72 (2013.01); C01P 2002/85 (2013.01); C01P 2004/04 (2013.01); C01P 2004/24 (2013.01); C01P 2004/64 (2013.01)] 12 Claims
OG exemplary drawing
 
1. A method for forming a mordenite (MOR) material, comprising:
combining N, N-trimethyl-1-1-adamantammonium (TMAda), at least one alcohol, a sodium source, an aluminum source, and a silica source at room temperature to form a synthesis mixture, wherein the N, N-trimethyl-1-1-adamantammonium (TMAda) and the at least one alcohol are combined to produce a synthesis mixture comprising an excess of the alcohol relative to the N, N-trimethyl-1-1-adamantammonium (TMAda);
maintaining the synthesis mixture for a time and at a temperature sufficient to allow mordenite (MOR) material to form; and
separating the mordenite (MOR) material from the synthesis mixture.