CPC C07C 51/12 (2013.01) [B01J 19/0006 (2013.01); C07C 51/44 (2013.01); B01J 2219/00162 (2013.01); B01J 2219/00164 (2013.01); C07C 53/08 (2013.01)] | 14 Claims |
1. A process for producing acetic acid comprising:
introducing methanol to a reactor at a first mass flow rate;
carbonylating the methanol in the reactor in the presence of a metal catalyst, iodide salt, water, and methyl iodide to form a reaction medium comprising acetic acid;
separating the reaction medium in a flash vessel into a liquid recycle stream and a vapor product stream comprising acetic acid, wherein the reaction medium is withdrawn at a second mass flow rate; and
adjusting the internal pressure of the flash vessel to maintain a mass flow ratio of the second mass flow rate to the first mass flow rate of less than or equal to 10.
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