US 11,940,214 B1
Freeze-dried product
Shuji Morimoto, Osaka (JP); Makoto Takehara, Tokyo (JP); and Masato Kobayashi, Osaka (JP)
Assigned to MII, LTD., Osaka (JP)
Appl. No. 18/284,291
Filed by MII LTD., Osaka (JP)
PCT Filed Aug. 2, 2022, PCT No. PCT/JP2022/029630
§ 371(c)(1), (2) Date Sep. 27, 2023,
PCT Pub. No. WO2023/013630, PCT Pub. Date Feb. 9, 2023.
Claims priority of application No. 2021-127617 (JP), filed on Aug. 3, 2021.
Int. Cl. F26B 5/06 (2006.01); F26B 17/20 (2006.01)
CPC F26B 5/065 (2013.01) [F26B 17/20 (2013.01)] 6 Claims
OG exemplary drawing
 
1. A freeze-dried product manufactured by being dried while moving in a state of receiving a mechanical force in a freeze-drying apparatus, wherein
the freeze-drying apparatus includes: a freezing unit for producing a frozen substance by spraying a raw material solution; and a drying unit for drying the frozen substance while transferring the frozen substance,
the freezing unit is configured to produce the frozen substance by discharging the raw material solution from a nozzle into a vacuum or into a cold air blowing environment,
the drying unit has a tubular shape linearly extending in a horizontal direction, the drying unit includes a tubular member kept in a vacuum state,
a spiral wall or groove portion is formed on an inner wall of the tubular member continuously in a longitudinal direction of the tubular member,
the drying unit is divided into three or more sections in the longitudinal direction to surround a periphery of the tubular member,
a temperature-controlled air or liquid is configured to be supplied to each of the three or more sections of the periphery of the tubular member to transfer a heat to the inner wall of the tubular member and the spiral wall or groove portion,
the tubular member is configured to be rotated to transfer the frozen substance or the freeze-dried product in the longitudinal direction of the tubular member while sliding on the spiral wall or groove portion, sublimate or dry the frozen substance or the freeze-dried product while transmitting the heat to the frozen substance or the freeze-dried product from the inner wall of the tubular member and the spiral wall or groove portion, and discharge a moisture evaporated when the frozen substance or the freeze-dried product is sublimated or dried to an outside,
a flow-start angle is less than 44 degrees or a repose angle is less than 55 degrees and larger than the flow-start angle, and
a residual amount is 3 g or less with respect to 10 g of the raw material solution fed into freeze-drying apparatus when a length of the tubular member is 30 cm in the longitudinal direction.