US 11,915,861 B2
Method for manufacturing rare earth permanent magnet
Dong Hwan Kim, Daegu (KR); and Koon Seung Kong, Daegu (KR)
Assigned to STAR GROUP IND. CO., LTD, Daegu (KR)
Appl. No. 16/975,886
Filed by STAR GROUP IND. CO., LTD, Daegu (KR)
PCT Filed Sep. 13, 2018, PCT No. PCT/KR2018/010755
§ 371(c)(1), (2) Date Aug. 26, 2020,
PCT Pub. No. WO2019/212101, PCT Pub. Date Nov. 7, 2019.
Claims priority of application No. 10-2018-0050000 (KR), filed on Apr. 30, 2018.
Prior Publication US 2021/0005380 A1, Jan. 7, 2021
Int. Cl. H01F 41/02 (2006.01); B22F 3/16 (2006.01); B22F 3/24 (2006.01); B22F 9/04 (2006.01); C22C 38/00 (2006.01); H02K 1/02 (2006.01)
CPC H01F 41/0293 (2013.01) [B22F 3/16 (2013.01); B22F 3/24 (2013.01); B22F 9/04 (2013.01); C22C 38/005 (2013.01); B22F 2003/248 (2013.01); B22F 2009/044 (2013.01); B22F 2201/10 (2013.01); B22F 2201/20 (2013.01); B22F 2202/05 (2013.01); B22F 2301/355 (2013.01); B22F 2304/10 (2013.01); C22C 2202/02 (2013.01); H02K 1/02 (2013.01)] 1 Claim
OG exemplary drawing
 
1. A method for manufacturing a rare earth sintered magnet comprising the steps of:
preparing a rare earth alloy composed of xwt % RE-ywt % B-zwt % TM-bal.wt % Fe, wherein RE is a rare earth element, TM is a 3d transition element, x=28˜35, y=0.5˜1.5, z=0˜15, and pulverizing the prepared rare earth alloy to a size of 1.0˜5.0 μm;
preparing heavy rare earth compounds and a heavy rare earth metal alloy and pulverizing the heavy rare earth compounds and the heavy rare earth metal alloy to a size of 1.0˜5.0 μm;
mixing the heavy rare earth compound powder of 40˜60 wt % with the heavy rare earth metal alloy powder of 40˜60 wt %;
mulling the pulverized rare earth alloy powder and the heavy rare earth compound powder and the heavy rare earth metal alloy powder at a ratio of 98-99 wt % pulverized rare earth alloy powder: 1-2 wt % heavy rare earth compound powder and heavy rare earth metal alloy powder, to be mixed;
aligning and compacting the mixed powder in a magnetic field, to be magnetized;
loading the magnetized mixture powder into a heating furnace and diffusing heavy rare earth elements of the heavy rare earth compounds and the heavy rare earth metal alloy to a grain boundary of the rare earth alloy under a vacuum or in an inert gas atmosphere;
sintering the powder of the rare earth alloy with the diffused heavy rare earth elements; and
performing a heat treatment to the sintered alloy,
wherein the heavy rare earth compounds are Gd-Hydride and one of the compounds which are Ho-Hydride, Dy-Hydride and Tb-Hydride as powders, and
wherein the heavy rare earth metal alloy is one of the alloys which are Gd-Al, Gd-Cu and Gd-Ag.