US 11,891,693 B2
Systems and methods for controlling vapor phase processing
Jereld Lee Winkler, Gilbert, AZ (US); Cheuk Li, Chandler, AZ (US); Michael F. Schultz, Mesa, AZ (US); and John Kevin Shugrue, Phoenix, AZ (US)
Assigned to ASM IP Holding B.V., Almere (NL)
Filed by ASM IP HOLDING B.V., Almere (NL)
Filed on Aug. 11, 2020, as Appl. No. 16/990,822.
Application 16/990,822 is a division of application No. 15/996,350, filed on Jun. 1, 2018, granted, now 10,774,422.
Prior Publication US 2020/0370179 A1, Nov. 26, 2020
Int. Cl. C23C 16/455 (2006.01); H01L 21/67 (2006.01); C23C 16/458 (2006.01); C23C 16/52 (2006.01)
CPC C23C 16/45544 (2013.01) [C23C 16/4583 (2013.01); C23C 16/52 (2013.01); H01L 21/67017 (2013.01)] 6 Claims
OG exemplary drawing
 
1. A method of controlling an atomic layer deposition (ALD) device comprising a reaction chamber, an exhaust line connected to the reaction chamber that transfers gas out of the reaction chamber, a valve along the exhaust line, a susceptor configured to support a substrate, a loading chamber below the reaction chamber, a partition separating the loading chamber from the reaction chamber, an inlet manifold connected to the reaction chamber, and a lower chamber pressure transducer exposed to the loading chamber, the method comprising:
controlling a dose state and a purge state of the ALD device according to an open loop control scheme, comprising:
forming a stored look-up table (LUT), comprising:
positioning the susceptor in the loading chamber such that the loading chamber is in fluid communication with the reaction chamber, and
for the plurality of preset gas loads along the exhaust line, measuring pressures in the loading chamber for a plurality of set points of the valve;
accessing the stored look up table (LUT), the LUT comprising a plurality of predetermined flow conductance settings of the valve corresponding to a non-zero flow conductance, a plurality of associated preset gas loads and a plurality of associated pressure values;
for the dose state of the ALD device, selecting a predetermined first non-zero flow conductance setting from the plurality of predetermined flow conductance settings of the valve corresponding to a first non-zero flow conductance based at least in part on a first desired pressure in the reaction chamber and a preset first gas load, from the plurality of preset gas loads, and sending a first signal to the valve corresponding to the selected first non-zero flow conductance setting, for the dose state;
for a purge state of the ALD device, selecting a predetermined second non-zero flow conductance setting from the plurality of predetermined flow conductance settings of the valve corresponding to a second non-zero flow conductance based at least in part on a second desired pressure in the reaction chamber and a preset second gas load, from the plurality of preset gas loads, and sending a second signal to the valve corresponding to the selected second non-zero flow conductance setting, wherein the first signal is different from the second signal, for the purge state;
placing the valve at the selected first non-zero flow conductance setting for at least a portion of the dose state;
pulsing a first reactant vapor into the reaction chamber during the dose state;
placing the valve at the selected second non-zero flow conductance setting for at least a portion of the purge state; and
purging the reaction chamber by supplying an inactive gas to the reaction chamber during the purge state.